蔬菜中西维因农药残留监测用荧光光谱仪的研究

王玉田; 王忠东

蔬菜中西维因农药残留监测用荧光光谱仪的研究

王玉田^1, ,,
王忠东^1,2

燕山大学电气工程学院,河北秦皇岛0660042.大庆石油学院分院,河北秦皇岛066004

详细信息

通讯作者:
王玉田

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出版历程
- 刊出日期: 2005-09-09

Study on Fluorescence Spectrometer for Monitoring Pesticide Residues in Vegetables

WANG Yu-tian^1, ,,
WANG Zhong-dong^1,2

Yanshan University,inhuangdao 066004,China;

More Information

Corresponding author:
WANG Yu-tian

摘要

摘要: 根据西维因农药受到紫外光激发能够发出荧光的特征，利用脉冲氙灯作为激发光源，利用光纤进行传输和探测荧光，并结合电荷耦合器件(CCD)光谱探测技术，设计出了一套能够测量农药含量的荧光光谱仪器。分别利用稳态光谱仪和该仪器实现了对黄瓜中西维因农药残留的快速测定。实验结果表明，在激发波长为319nm和荧光发射波长为647nm情况下，西维因的线性范围为0.0～120μg／L，最低检出限LOD为5×10-7μg/L,线性相关系数r为0.9991(S／N=5)。该仪器可满足荧光检测的需要。
- 西维因 /
- 农药残留 /
- 荧光光谱 /
- 光纤传感 /
- 仪器设计
Abstract: A fluorescence spectrometer which can measure pesticide concentration is designed by using a xenon lamp as excitation lightsource，employing optical fibers to transmit and detect fluorescence and combining with CCD spectrumdetermination technology based on fluorescent characteristics of carbaryl that can emit fluorescence as it is excited by UV rays.Moreover,the rapid measurement of carbaryl residues in cucumbers is implemented with a steadystate fluorescent spectrograph and the new system respectively. The results indicate that the linear concentration range is 0.0～120.0μg／L for carbaryl, the detection limit (LOD) is 5×10-7μg／L，the linear correlation coefficient r is 0.9991 as the excitation wavelength is 319nm and the fluorescence emission wavelength is 647nm. The data prove up to the hilt that the instrument meets the demand of fluorescence detection.
- carbaryl /
- pesticide residue /
- fluorescence spectrum /
- optical fiber sensing /
- instrument design