可见近红外波长标准物质的研制

Development of visible near-infrared wavelength reference materials

  • 摘要: 为拓宽标准物质波段范围,采用物化性能稳定的掺杂有镨钕稀土元素的玻璃作为可见波长的标准物质的原材料,同时采用物化性能稳定的聚苯乙烯片(厚度1 mm)作为近红外波长的标准物质的原材料,利用二者互不影响的特点,并且将其叠加使用会拓展波段范围,由此研制了可见近红外波长标准物质。以F检验法对样品的均匀性进行了检验,用线性拟合法对样品的稳定性进行考察,通过溯源至国家基标准的方式解决了溯源性,确定了标准物质中的波段范围为430 nm~2 550 nm,不确定度为0.1 nm~1.0 nm。弥补了当前标准物质中波段范围覆盖太窄的缺陷。

     

    Abstract: In order to broaden the wavelength range of the standards, the glass doped with praseodymium and neodymium rare earth elements with stable physical and chemical properties was used as the raw material of the visible wavelength reference material. At the same time, the polystyrene sheet (thickness of 1 mm) with stable physical and chemical properties was used as the raw material of the near-infrared wavelength reference material. The visible and near-infrared wavelength reference material was developed by using the characteristics that the two did not affect each other, and the superposition of the two would expand the band range. The uniformity of the sample was tested by F test method, and the stability of the sample was investigated by linear fitting method. The traceability was solved by tracing to the national standard. The band range of standard material was determined to be 430 nm~2 550 nm, and the uncertainty was 0.1 nm~1.0 nm, which made up for the defect that the wave range coverage in the current reference material is too narrow.

     

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