基于椭圆偏振显微镜的纳米级磁头润滑膜观测方法

刘卿卿, 苏杨

刘卿卿, 苏杨. 基于椭圆偏振显微镜的纳米级磁头润滑膜观测方法[J]. 应用光学, 2017, 38(3): 434-437. DOI: 10.5768/JAO201738.0303001
引用本文: 刘卿卿, 苏杨. 基于椭圆偏振显微镜的纳米级磁头润滑膜观测方法[J]. 应用光学, 2017, 38(3): 434-437. DOI: 10.5768/JAO201738.0303001
Liu Qingqing, Su Yang. Visualization of nanometer head slider lubricant films based on ellipsometric microscope[J]. Journal of Applied Optics, 2017, 38(3): 434-437. DOI: 10.5768/JAO201738.0303001
Citation: Liu Qingqing, Su Yang. Visualization of nanometer head slider lubricant films based on ellipsometric microscope[J]. Journal of Applied Optics, 2017, 38(3): 434-437. DOI: 10.5768/JAO201738.0303001

基于椭圆偏振显微镜的纳米级磁头润滑膜观测方法

基金项目: 

江苏省自然科学基金 BK20130989

南京信息工程大学引进人才启动基金 2013R106

详细信息
    作者简介:

    刘卿卿(1983-),女,辽宁海城人,博士,讲师,主要从事光学仪器及光电检测方向技术研究。Email:sherryliuqq@163.com

  • 中图分类号: TH742

Visualization of nanometer head slider lubricant films based on ellipsometric microscope

  • 摘要: 针对磁头飞行导致液体润滑膜的转移研究以及润滑膜在磁头上的动态变化特性观测问题,基于改进的垂直物镜的椭圆偏振显微镜,提出起偏器相移方法的磁头表面润滑膜厚度计算模型,实现了润滑膜厚度的测量。实验以非极性润滑剂Z03覆盖的磁头为样品对椭圆偏振显微镜进行标定,以极性润滑剂Zdol4000作为样品,对其在磁头表面的去湿现象进行观察。该方法测量精度可达0.37 nm,分辨力约0.36 μm,可为其他纳米级薄膜观测提供一定的技术参考。
    Abstract: Aiming at the problems of shift of lubricant films on head slider, and dynamic change visualization of lubricant films on head slider, this paper presents caculation model of lubricant thickness distribution on a head slider surface using phase shift method, which is base on improved vertical-objective-based ellipsometric microscope (VEM). Measurement of lubricant film thickness is achived with this method. Taking nonpolar perfluoropolyether (PFPE) lubricant Z03 as a sample, ellipsometric microscope is calibrated; while taking polar PFPE lubricant Zdol4000 as a sample, dewetting on head slider surface is observed. Experimental results show measuring accuracy and resolution are 0.37 nm and 0.36 μm respectively. This can be reference for other visualization of nm lubricant films.
  • 图  1   椭偏参量相位差|Δ-Δd|与膜厚h近似线性关系

    Figure  1.   Linear relationship of phase shift |Δ-Δd| and thickness h.

    图  2   VEM结构示意图

    Figure  2.   Schematic of VEM.

    图  3   VEM标定结果

    Figure  3.   Calibration results of VEM.

    图  4   刀口目标成像法所得VEM的MTF曲线

    Figure  4.   MTF of VEM obtained from observation of the knife-edge image

    图  5   磁头润滑膜去湿现象观测,h=6.7 nm

    Figure  5.   Dewetting image of lubricant film on head slider at different times, h=6.7 nm.

  • [1] 潘登, 闫辉, 姜洪源.磁头/磁盘间润滑剂转移机理及影响因素[J].物理学报, 2014, 63(12): 128104. doi: 10.7498/aps.63.128104

    Pan Deng, Yan Hui, Jiang Hongyuan. Lubricant transfer mechanism and process between slider and disk[J]. Acta Phys. Sin., 2014, 63(12): 128104. doi: 10.7498/aps.63.128104

    [2]

    Tani H, Koganezawa S, Tagawa N. Reduction in lubricant pickup by bias voltage between slider and disk surfaces[J]. Microsystem Technologies, 2016, 22(6):1221-1225. doi: 10.1007/s00542-016-2814-6

    [3] 史宝军, 季家东, 杨廷毅.表面粗糙度对硬盘超低飞高气膜静态特性的影响[J].机械工程学报, 2011, 47(11):93-99. http://d.old.wanfangdata.com.cn/Periodical/jxgcxb201111015

    Shi Baojun, Ji Jiadong, Yang Tingyi. Effects of surface roughness on static characteristics of air bearing films in hard disk drives with ultra-low flying heights[J].Journal of mechanical engineering, 2011, 47(11): 93-99. http://d.old.wanfangdata.com.cn/Periodical/jxgcxb201111015

    [4] 王益朋.薄膜厚度的椭圆偏振光法测量[D].天津: 天津大学, 2010.

    Wang Yipeng. Film thickness measurement based on ellipsometry[D]. Tianjin: Tianjin University, 2010.

    [5] 李倩, 杭凌侠, 徐均琪. UBMS技术制备DLC薄膜的光学常数椭偏分析[J].应用光学, 2009, 30(1): 105-109. doi: 10.3969/j.issn.1002-2082.2009.01.025

    Li Qian, Hang Lingxia, Xu Junqi. Ellipsometric analysis of optical constants for diamond-like carbon films deposited by UBMS[J]. Journal of Applied Optics, 2009, 30(1): 105-109. doi: 10.3969/j.issn.1002-2082.2009.01.025

    [6]

    Henon S, Meunier J. Microscope at the brewster angle: direct observation of first-order phase transitions in monolayers[J]. Rev. Sci. Instrum, 1991, 62(4): 936-939. doi: 10.1063/1.1142032

    [7]

    Kajihara Y, Fukuzawa K, Itoh S, et al. Theoretical and experimental study on two-stage-imaging microscopy using ellipsometric contrast for real-time visualization of molecularly thin films[J]. Rev. Sci. Instrum., 2013, 84(5): 053704. doi: 10.1063/1.4804633

    [8]

    Neumaier K R, Elender G, Sackmann E, et al. Ellipsometric microscopy[J], Europhys. Lett., 2000, 49(1): 14-19. doi: 10.1209/epl/i2000-00113-x

    [9]

    Fukuzawa K, Liu Q, Tarukado T, et al. Novel methods for real-time observation of molecularly thin lubricant films by ellipsometric microscopy: application to dewetting observation[J]. IEEE Trans. magn., 2013, 49(6): 2530-2534. doi: 10.1109/TMAG.2013.2247580

    [10]

    Azzam R M A, Bashara N M. Ellipsometry and polarized light[M]. Amsterdam: North Holland, 1986.

    [11]

    Fukuzawa K, Noda T, Mitsuya Y. Direct visualization of molecularly thin lubricant films on magnetic disks with a digitally enhanced ellipsometric microscope[J]. IEEE Trans. Magn., 2003, 39(2): 898-902. doi: 10.1109/TMAG.2003.808917

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出版历程
  • 收稿日期:  2016-08-21
  • 修回日期:  2016-11-13
  • 刊出日期:  2017-04-30

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